SAXS and XRD studies on the microstructure of TiO2 nanoparticles | Zendy

Zhongjun Chen | Zendy; Wei Wang | Zendy; Quan Cai | Zendy; Chen Xing | Zendy; Zhonghua Wu | Zendy; Li Rong-Ping | Zendy; Che Chuan-Qiang | Zendy; Pan Wei | Zendy

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SAXS and XRD studies on the microstructure of TiO2 nanoparticles

Author(s) -

Zhongjun Chen,

Wei Wang,

Quan Cai,

Chen Xing,

Zhonghua Wu,

Li Rong-Ping,

Che Chuan-Qiang,

Pan Wei

Publication year - 2008

Publication title -

acta physica sinica

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.199

H-Index - 47

ISSN - 1000-3290

DOI - 10.7498/aps.57.5793

Subject(s) - small angle x ray scattering , materials science , nanoparticle , synchrotron radiation , annealing (glass) , microstructure , phase transition , chemical engineering , sol gel , phase (matter) , scattering , nanotechnology , composite material , optics , thermodynamics , chemistry , physics , engineering , organic chemistry

TiO2 nanoparticles were prepared by sol-gel methodand were annealed at different temperatures from 300 to 800℃. Their interfacial and fractal characteristics as well as and phase transition were investigated by using synchrotron radiation SAXS and XRD techniques. The change of nanoparticle size with annealing temperature was determined. The relationship between the interfacial characteristics and phase transition was discussed in this paper.

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