Open AccessEffects of annealing of r-cut sapphire substrate on its surface morphology and the growth of CeO2 buffer layers and the Tl-2212 superconducting films
Author(s) -
Xie Qing-lian,
Yan Shao-lin,
Xinjie Zhao,
Fang Lan,
Ji Lin Lu,
Yuting Zhang,
You Shi-Tou,
Li Jia-Lei,
Zhenming Xu,
Tiege Zhou,
Zuo Tao,
Hongwei Yue
Publication year - 2008
Publication title -
wuli xuebao
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.199
H-Index - 47
ISSN - 1000-3290
DOI - 10.7498/aps.57.519
Subject(s) - annealing (glass) , materials science , sapphire , atomic force microscopy , superconductivity , analytical chemistry (journal) , composite material , condensed matter physics , nanotechnology , optics , chemistry , laser , physics , chromatography
In this study, the surface morphology evolution and the change of the phase structure of r-cut sapphire substrates annealed at different temperatures for different time in O2, and the effects of annealing conditions on the growth of CeO2 and Tl-2212 films, were investigated by AFM and XRD. The results of AFM show that the local steps on the substrate annealed at 1000℃ is formed firstly, and then the multilayer terrace-and-step structure, yielding from prolonging annealing time, evolves into wide terrace-and-step structure with ultrasmooth terrace through the coalition of initial localized steps, which slightly tilts to the surface. XRD measurements show that the CeO2 films prepared on r-cut sapphire annealed at the optimized conditions and the 500 nm thick Tl-2212 films grown on the CeO2 buffer layers subsequently possess excellent in-plane and out-of plane orientation, and the annealing temperature and annealing time have strong effect on the crystalline quality of substrates and CeO2 films. The Tl-2212 films have a high transition temperature (Tc=104.7 K), a high critical current density (Jc=3.5 MA/cm2 at 77.3K and zero applied magnetic field) and a low surface resistance (Rs=390μΩ at 10GHz and 77K).