DETERMINATION OF CRYSTAL STRUCTURE OF α-CHLORO-N-SEC-BUTYI-CINNAMIDE | Zendy

ZHENG CHAO-DE | Zendy; GU YUAN-XIN | Zendy

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DETERMINATION OF CRYSTAL STRUCTURE OF α-CHLORO-N-SEC-BUTYI-CINNAMIDE

Author(s) -

ZHENG CHAO-DE,

GU YUAN-XIN

Publication year - 1983

Publication title -

acta physica sinica

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.199

H-Index - 47

ISSN - 1000-3290

DOI - 10.7498/aps.32.280

Subject(s) - diffractometer , orthorhombic crystal system , crystal structure , dimension (graph theory) , crystal (programming language) , crystallography , intensity (physics) , molecule , matrix (chemical analysis) , block (permutation group theory) , physics , materials science , combinatorics , mathematics , optics , computer science , chemistry , quantum mechanics , composite material , programming language

α-CHLORO-N-SEC-BUTYI-CINNAMIDE crystal (trans) belongs to orthorhombic system. The space group is D2h15-Pbca with eight molecules in a cell of dimension α= 18.842 (0.006)?, b=14.076 (0.006)?, c=10.077 (0.003)?. The intensity data were collected on RASA-IIS four-circle diffractometer. The number of independent reflexions is 929. The structure was solved by direct method (MULTAN-80). Refinement of structure parameters was achieved by block- matrix least-squares method, R =0.088.

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