THE CRYSTAL STRUCTURE OF METHOXY-FORMYL-TRICHLOROACETYL-METHYLENE-PHOSPHORUS (YLID-IV) | Zendy

Cun-Heng He | Zendy; ZHENG QI-TAI | Zendy; SHEN FU-LING | Zendy; Shi-qi Dou | Zendy; Lin Guangda | Zendy

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THE CRYSTAL STRUCTURE OF METHOXY-FORMYL-TRICHLOROACETYL-METHYLENE-PHOSPHORUS (YLID-IV)

Author(s) -

Cun-Heng He,

ZHENG QI-TAI,

SHEN FU-LING,

Shi-qi Dou,

Lin Guangda

Publication year - 1982

Publication title -

acta physica sinica

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.199

H-Index - 47

ISSN - 1000-3290

DOI - 10.7498/aps.31.825

Subject(s) - monoclinic crystal system , crystal (programming language) , crystal structure , methylene , crystallography , physics , chemistry , materials science , medicinal chemistry , computer science , programming language

The YLID-IV (C22H18O3PCl3) crystal belongs to the monoclinic system with space group P21/n and unit cell parameter α = 13.518(6)?, b = 14.923(7)?, c = 11.473(5)?, β = 99.81(2), z = 4. The intensity data were collected on the Philips PW-1100 diffrac-tometer. The structure was determined by direct method (MULTAN-78) and refined by full-matrix least-squares method to a final R value of 0.074 for 2592 reflexions. The hydrogen atom locations were determined by difference Fourier synthesis.

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