DEVELOPMENT OF REACTOR-TYPE "DIP CATALYST" FOR TRANSITION METAL NANOPARTICLE-EMBEDDED POLYMER THIN FILMS | Zendy

Deyvid G. M. Oliveira | Zendy; Glademir Alvarenga | Zendy; Carla Weber Scheeren | Zendy; Gilber R. Rosa | Zendy

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DEVELOPMENT OF REACTOR-TYPE "DIP CATALYST" FOR TRANSITION METAL NANOPARTICLE-EMBEDDED POLYMER THIN FILMS

Author(s) -

Deyvid G. M. Oliveira,

Glademir Alvarenga,

Carla Weber Scheeren,

Gilber R. Rosa

Publication year - 2014

Publication title -

química nova

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.214

H-Index - 73

eISSN - 1678-7064

pISSN - 0100-4042

DOI - 10.5935/0100-4042.20140224

Subject(s) - nanoparticle , materials science , catalysis , polymer , transition metal , thin film , nanotechnology , chemical engineering , composite material , chemistry , organic chemistry , engineering

This article describes the development of a new catalytic reactor designed to operate with nanoparticle-embedded polymer thin films. Stabilization of metal nanoparticles in films that serve as catalysts in organic reactions is relatively new; therefore, the development of reactors to facilitate their use is necessary. We describe in detail the preparation of the GDCR reactor-type "dip catalyst" and its evaluation in the Suzuki - Miyaura cross-coupling reaction of phenylboronic acid and 4-bromoanisole catalyzed by palladium nanoparticle-embedded cellulose acetate thin film (CA/PD(0)). Compared with earlier prototypes, GDCR reactor showed excellent results when operating with CA/PD(0) thin films

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