Open AccessA REPORT ABOUT BENZOXAZINONE MATERIAL
Author(s) -
Abdul Ahad
Publication year - 2020
Publication title -
chemistry and material sciences research journal
Language(s) - English
Resource type - Journals
eISSN - 2708-8626
pISSN - 2708-8618
DOI - 10.51594/cmsrj.v2i1.91
Subject(s) - triethylamine , piperazine , dichloromethane , melting point , reagent , phenol , chemistry , chloride , benzoyl chloride , combinatorial chemistry , substitution (logic) , organic chemistry , nuclear chemistry , computer science , solvent , programming language
In this study, the objective was to investigate the Benzoxazinone material using the uncorrected and open capillary method for conducting and reporting the melting points. Laboratory grade and analytical grade reagents were used for conducting the synthesis and analytical studies based on with or without modification appropriately as and were required. Results showed that First of all the Synthesis of 2H-1, 4- benzoxazin-3(4H)-one was carried out by reacting 2- amino phenol with chloro acetyl chloride in dichloromethane in presence of triethylamine and then the bromo substitution was done by reacting with dibromoethane. Piperazine substituents were prepared in laboratory and then the title compounds were synthesized. One additional benzoyl substitution was also done. The entire synthesized compounds were primarily characterized by running T.L.C. and melting point analysis.