Open AccessSynthesis and characterisation of some mixed ligands adducts of benzoylacetone and salicylaldehyde
Author(s) -
Adamu Mustapha,
Muhammad Saleh Salga,
Sani Sabo
Publication year - 2018
Publication title -
bayero journal of pure and applied sciences
Language(s) - English
Resource type - Journals
ISSN - 2006-6996
DOI - 10.4314/bajopas.v11i1.29
Subject(s) - salicylaldehyde , adduct , chemistry , metal , ligand (biochemistry) , thermal decomposition , thermal stability , decomposition , photochemistry , polymer chemistry , organic chemistry , schiff base , biochemistry , receptor
A series of four mixed ligand complexes were synthesized by reacting benzoylacetone and salicylaldehyde with different metal chlorides in ethanolic medium. The complexes have been characterized by molar conductance measurements and spectral techniques such as IR and Uv-visible electronic spectra. Decomposition temperature was also determined. The results indicated that the compounds have bands at 400-500cm-1, with very sharp melting points. This proved the formation of metal-oxygen bond, purity and high thermal stability of the compounds that could lead to a high antimicrobial activity.Keywords: Adduct Synthesis, Ligands, and Complexes