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Green Synthesis of Silver Nanoparticles Using Hibiscus sabdariffa Leaves Extract
Author(s) -
Siti Husnaa Mohd Taib,
Kamyar Shameli,
Roshafima Rasit Ali,
Zahra Izadiyan,
Zatil Izzah Tarmizi
Publication year - 2021
Publication title -
journal of research in nanoscience and nanotechnology
Language(s) - English
Resource type - Journals
ISSN - 2773-6180
DOI - 10.37934/jrnn.3.1.7681
Subject(s) - hibiscus sabdariffa , fourier transform infrared spectroscopy , nanoparticle , nuclear chemistry , silver nanoparticle , transmission electron microscopy , spectroscopy , materials science , biomolecule , chemistry , ultraviolet visible spectroscopy , analytical chemistry (journal) , chemical engineering , nanotechnology , organic chemistry , physics , food science , quantum mechanics , engineering
The present paper reports the synthesis of silver nanoparticles (Ag-NPs) by a green method using Hibiscus sabdariffa (H. sabdariffa) leaves extract as reductant and stabilizer. The synthesized Ag-NPs were characterized by ultraviolet-visible (UV-vis) spectroscopy, transmission electron microscopy (TEM), atomic force microscopy (AFM) and Fourier transform infrared spectroscopy (FTIR). UV-vis spectrum of synthesized Ag-NPs showed a peak at 378 nm. TEM analysis revealed that the particles were spherical and irregular in shape and has average size around 56.52 nm. This structure and size of particles were confirmed by AFM analysis. The UV-vis and FTIR spectrum provides evidence of the presence of caffeic acid component as a representative biomolecule in stabilising the nanoparticles based on previous studies. Hence, this study advocates that H. sabdariffa have potential for synthesizing nanoparticles.

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