Open AccessStudy the impact of different preparation methods on the structural and dielectric properties of nickel-zinc ferrite
Author(s) -
Marwa Taha Jasim,
Tahseen H. Mubarak,
Abdul Samee F. Abdul Aziz
Publication year - 2021
Publication title -
sustainable engineering and innovation
Language(s) - English
Resource type - Journals
ISSN - 2712-0562
DOI - 10.37868/sei.v3i2.id117
Subject(s) - spinel , fourier transform infrared spectroscopy , materials science , dielectric , analytical chemistry (journal) , zinc ferrite , ferrite (magnet) , nickel , zinc , dielectric loss , infrared spectroscopy , spectroscopy , metallurgy , chemical engineering , chemistry , composite material , chromatography , physics , optoelectronics , organic chemistry , quantum mechanics , engineering
In the current study, nickel-zinc ferrite nanoparticles Ni (1-x) ZnxFe2O4 (X= 0, 0.25, 0.50, 0.75, 1) have been arranged by sol-gel auto combustion and common chemical precipitation methods, The samples were described by x-ray (XRD) deflection, Fourier converts Infrared Spectroscopy (FTIR), dielectric perpetual and dielectric loss element. the XRD analysis confirms the cubic lone phase spinel configuration for all the synthesized materials. Average crystalline size is estimated of the (311) peaks of the x-ray diffractogram using Scherrer’s formulation institute in the range 38.90 to 37.71 nm for sol-gel auto burning method and from 18.61 to 23.41 nm for co-precipitation method. The Fourier transform infrared spectroscopy was studied so as to assert the construction of the spinel phase and to recognize the kind of carbon remaining in the samples. The dielectric fixed and the dielectric loss factor were measured in the range between 50 Hz – 3 MHz at room temperature were located to be reduced with a rise in regularity.