Open AccessIn-Situ Synthesis and Characterization of Schiff base [Zn(Anil-oPD)4] Metal Complex
Publication year - 2019
Publication title -
international journal of innovative technology and exploring engineering
Language(s) - English
Resource type - Journals
ISSN - 2278-3075
DOI - 10.35940/ijitee.b1138.1292s419
Subject(s) - schiff base , cyclic voltammetry , metal , fourier transform infrared spectroscopy , chemistry , nickel , nuclear chemistry , infrared spectroscopy , spectroscopy , inorganic chemistry , polymer chemistry , electrochemistry , organic chemistry , electrode , chemical engineering , physics , quantum mechanics , engineering
The insitu synthesis of Schiff base metal complex using o-phenylenediamine (oPD) and p-anisaldehyde (p-anisal) as starting materials with Nickel nitrate hexahydrate (Zn(NO3)2.6H2O) as a metal precursor in equimolar ratio (1:1:1 M) at room temperature. After the reaction time, the prepared metal complex washed several times with ethanol and boiled water for complete removal of un-reacted starting materials. The following characterization was used to confirm the metal complex by UV-visible spectroscopy (UV-Vis.), Fourier Transforms-Infrared spectroscopy (FT-IR), X-ray diffraction pattern (XRD) and Cyclic Voltammetry (CV).