Open AccessSingle Pot Synthesis, Characterization of Nickel Schiff Base Metal Complex by in-Situ Method
Publication year - 2019
Publication title -
international journal of innovative technology and exploring engineering
Language(s) - English
Resource type - Journals
ISSN - 2278-3075
DOI - 10.35940/ijitee.b1135.1292s419
Subject(s) - nickel , schiff base , cyclic voltammetry , metal , fourier transform infrared spectroscopy , chemistry , nuclear chemistry , inorganic chemistry , characterization (materials science) , infrared spectroscopy , materials science , polymer chemistry , electrochemistry , organic chemistry , nanotechnology , chemical engineering , electrode , engineering
The insitu synthesis of Schiff base metal complex using p-toluedine (p-tolu), p-anisaldehyde (p-anisal) as starting materials with Nickel nitrate hexahydrate (Ni(NO3)2.6H2O) used as a precursor for metal in equimolar ratio (1:1:1 M) at room temperature. The prepared metal complex is washed with several times with ethanol and boiled water for the complete removal of un-reacted species. To confirm the prepared material by the following characterization like UV-visible, Fourier Transforms Infrared spectroscopy, X-ray diffraction pattern and Cyclic Voltammetry.