
X-RAY SPECTRAL MICROANALYSIS OF ELECTROEROSIVE POWDER MATERIAL OBTAINED IN AN ETHYL ALCOHOL MEDIUM FROM WASTE OF A NON-TUNGSTEN HARD ALLOY OF THE KNT16 BRAND
Author(s) -
Е. В. Агеева,
B. N. Sabelnikov
Publication year - 2020
Publication title -
izvestiâ volgogradskogo gosudarstvennogo tehničeskogo universiteta
Language(s) - English
Resource type - Journals
ISSN - 1990-5297
DOI - 10.35211/1990-5297-2020-7-242-33-36
Subject(s) - tungsten , materials science , alloy , scanning electron microscope , microanalysis , metallurgy , dispersion (optics) , composite material , chemistry , optics , organic chemistry , physics
The first appearance of tungsten-free hard alloys (TFHA) was noted in the early 30s of the last century, but they did not receive due attention and, accordingly, spread due to insufficient strength and were replaced by tungsten-containing alloys of such groups as VK, TC and TTK. However, the rapidly developing shortage of expensive tungsten pushed in the late 50s to return to the search for hard alloys, the composition of which does not include tungsten. Due to the growing demand for tungsten-free hard alloys, the problem of recycling their waste with the possibility of reuse is acute in the industry. The purpose of this work was to conduct x-ray spectral microanalysis (RSMA) of powder material (PM) obtained by electroerosive dispersion (EED) in ethyl alcohol from waste of a non-tungsten hard alloy of the KNT16 brand. The resulting powder material was examined using an energy-dispersion x-ray analyzer from EDAX, built into a scanning electron microscope "QUANTA 600 FEG". In the course of scientific research, the spectra of characteristic x-ray radiation on the surface of the experimentally obtained sample were obtained. The results obtained in the course of scientific research can be used to create environmentally friendly resource-saving processes for processing waste of tungsten-free hard alloys into powder materials.