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Nanocrystals of Cs 2 SnX 6  (X = Cl, Br, Br 0.5 I 0.5 , and I) have been prepared by a simple, optimized, hot-injection method, reporting for the first time the synthesis of Cs 2 SnCl 6 , Cs 2 SnBr 6 , and mixed Cs 2 Sn(I 0.5 Br 0.5 ) 6  nanocrystalline samples. They all show a cubic crystal structure with a linear scaling of lattice parameter by changing the halide size. The prepared nanocrystals have spherical shape with average size from 3 to 6 nm depending on the nature of the halide and span an emission range from 444 nm (Cs 2 SnCl 6 ) to 790 nm (Cs 2 SnI 6 ) with a further modulation provided by mixed Br/I systems.

Highly Tunable Emission by Halide Engineering in Lead-Free Perovskite-Derivative Nanocrystals: The Cs2SnX6 (X = Cl, Br, Br/I, I) System