Open AccessA novel and facile method for silica nanoparticles synthesis from high temperature vulcanization (HTV) silicon
Author(s) -
Mohammad Senemar,
Ali Maleki,
Behzad Niroumand,
Alireza Allafchian
Publication year - 2016
Publication title -
metallurgical and materials engineering
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.161
H-Index - 2
eISSN - 2812-9105
pISSN - 2217-8961
DOI - 10.30544/134
Subject(s) - materials science , vulcanization , fourier transform infrared spectroscopy , nanoparticle , dynamic light scattering , transmission electron microscopy , amorphous solid , chemical engineering , silicon , scanning electron microscope , field electron emission , nanotechnology , composite material , organic chemistry , optoelectronics , natural rubber , electron , chemistry , engineering , physics , quantum mechanics
This study is introducing a facile and novel method for synthesis of amorphous silica nanoparticles. Silica nanoparticles were synthesized by pyrolysis and combustion of high temperature vulcanization (HTV) silicone at 700 oC for 1 h. The products were investigated employing transmission electron microscopy (TEM), field emission scanning electron microscopy (FESEM), dynamic light scattering (DLS), X-ray diffraction (XRD), Brunauer Emmett and Teller (BET) test and Fourier Transform Infrared (FTIR) Spectroscopy. The results indicated that the method is capable of synthesis of amorphous silica nanoparticles with sizes of mostly between 10 and 50 nm.