Open AccessSynthesis of spin-labeled emoxypine, methionine, o-anisidine
Author(s) -
M. V. Lisouskaya,
N. V. Kot
Publication year - 2020
Publication title -
vescì nacyânalʹnaj akadèmìì navuk belarusì. seryâ hìmìčnyh navuk
Language(s) - English
Resource type - Journals
eISSN - 2524-2342
pISSN - 1561-8331
DOI - 10.29235/1561-8331-2020-56-2-192-196
Subject(s) - electron paramagnetic resonance , spectroscopy , mass spectrometry , electron paramagnetic resonance spectroscopy , methionine , nuclear magnetic resonance spectroscopy , chemistry , infrared spectroscopy , site directed spin labeling , nuclear magnetic resonance , nuclear chemistry , analytical chemistry (journal) , amino acid , organic chemistry , chromatography , biochemistry , physics , quantum mechanics
Spin-labeled (acylated with 4-doxylpentanoic acid) emoxypine, methionine, o-anisidine were synthesized. The compounds obtained were characterized using nuclear magnetic resonance spectroscopy, electron paramagnetic resonance spectroscopy, infrared and ultraviolet spectroscopy and mass spectrometry. Synthesized spin-labeled compounds can be used for biochemical studies using EPR spectroscopy.