Open AccessTHERMOGRAVIMETRIC ANALYSIS OF NANO CRYSTALLINE CERAMIC PbSrCaCuO
Author(s) -
Reenu Jacob,
Jayakumari Isac
Publication year - 2014
Publication title -
journal of advances in chemistry
Language(s) - English
Resource type - Journals
ISSN - 2321-807X
DOI - 10.24297/jac.v10i7.6801
Subject(s) - thermogravimetric analysis , ceramic , materials science , homogeneity (statistics) , nano , ball mill , chemical engineering , solid state , high energy , elemental analysis , composite material , chemistry , computer science , engineering physics , inorganic chemistry , machine learning , engineering
Nano crystalline ceramic PbSrCaCuO was prepared by the solid state technique via a high-energy ball milling process through mechanically assisted synthesis.The prepared sample was then subjected to calcinations to acquire the desired homogeneity and phase formation. To establish the elemental composition EDX analysis was done.TGA and DTA were used to study the behaviour of the sample upon heating to a high temperature.