Nickel(II) cyclohexylethyl-dithiocarbamate P-donor ligands in the coordination sphere | Zendy

J. Husarek | Zendy; Richard Pstorek | Zendy; Michal Maloň | Zendy; Zedenek Sindalar | Zendy; M. Pavlicek | Zendy

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Nickel(II) cyclohexylethyl-dithiocarbamate P-donor ligands in the coordination sphere

Author(s) -

J. Husarek,

Richard Pstorek,

Michal Maloň,

Zedenek Sindalar,

M. Pavlicek

Publication year - 2004

Publication title -

journal of the serbian chemical society

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.227

H-Index - 45

eISSN - 1820-7421

pISSN - 0352-5139

DOI - 10.2298/jsc0412053h

Subject(s) - dithiocarbamate , nickel , chemistry , diamagnetism , spectroscopy , coordination complex , chromophore , elemental analysis , inorganic chemistry , infrared spectroscopy , conductivity , coordination sphere , crystallography , metal , photochemistry , organic chemistry , magnetic field , crystal structure , physics , quantum mechanics

A series of new Ni(II) dithiocarbamate compounds of the composition [NiX(cetdtc)(PR3)](X = Cl, Br, I, NCS; cetdtc = cyclohexylethyldithiocarbamate; R = phenyl, n-butyl) has been synthesized. All the isolated complexes have been characterized by elemental analysis, IR and UV/VIS spectroscopy, 31P{1H}-NMR spectroscopy, thermal analysis magnetochemical and conductivity measurements. On the basis of the results of the physico-chemical study, all complexes are diamagnetic, non-electrolytes with a square-planar NiS2PX chromophore.

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