Open AccessMetal complexes of 3-chloro-4-hydrazino-carbonyl-methoxy-benzenesulfondibuthylamide
Author(s) -
Anca Mihaela Mocanu,
Corina Cernătescu
Publication year - 2008
Publication title -
chemical industry and chemical engineering quarterly
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.189
H-Index - 26
eISSN - 2217-7434
pISSN - 1451-9372
DOI - 10.2298/ciceq0801001m
Subject(s) - recrystallization (geology) , metal , solvent , organic solvent , hydrazide , ethanol , chemistry , metal carbonyl , elemental analysis , inorganic chemistry , transition metal , nuclear chemistry , materials science , organic chemistry , chemical engineering , catalysis , paleontology , engineering , biology
By taking the biological activity of 3-chloro-4-hydrazinocarbonyl-methoxy-benzenesulphondibuthylamide and of some transitional metals (Cu, Co, Cr, Fe, Mn, Ni, Sn) into account we considered it useful to capitalize the already obtained hydrazide by complexion reactions with various metallic salts. The reaction was carried out in the organic solvent medium, by heating under stirring. The obtained products were purified by recrystallization from organic solvents (especially ethanol) and characterized by means of melting points, elemental analysis and spectral measurements.