
Preparation and investigation of the properties of hexanitrohexaazatricyclododecanidione (HHTDD)
Author(s) -
Mateusz Szala,
L. Szymańczyk
Publication year - 2019
Publication title -
materiały wysokoenergetyczne
Language(s) - English
Resource type - Journals
ISSN - 2083-0165
DOI - 10.22211/matwys/0057e
Subject(s) - standard enthalpy change of formation , enthalpy , sensitivity (control systems) , materials science , combustion , heat of combustion , qualitative analysis , thermodynamics , chemistry , engineering , physics , qualitative research , electronic engineering , social science , sociology
Literature descriptions of methods for obtaining hexanitrohexaazatricyclododecanedione are discussed. The most advantageous method for preparing the compound on a laboratory scale was selected for experimental research. A full structural and qualitative analysis of the final product was carried out. The heat of combustion was determined calorimetrically and the standard enthalpy of HHTDD formation was calculated based on this value. The sensitivity of the material to mechanical stimuli (impact and friction) was determined.