RAPID SOLVENT-FREE MICROWAVE ASSISTED SYNTHESIS OF SOME N’-BENZYLIDENE SALICYLIC ACID HYDRAZIDES | Zendy

Tutuk Budiati | Zendy; Stephanie D.A. | Zendy; Elisabeth Catherina Widjajakusuma | Zendy

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RAPID SOLVENT-FREE MICROWAVE ASSISTED SYNTHESIS OF SOME N’-BENZYLIDENE SALICYLIC ACID HYDRAZIDES

Author(s) -

Tutuk Budiati,

Stephanie D.A.,

Elisabeth Catherina Widjajakusuma

Publication year - 2012

Publication title -

indonesian journal of chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.273

H-Index - 14

eISSN - 2460-1578

pISSN - 1411-9420

DOI - 10.22146/ijc.21357

Subject(s) - chemistry , microwave irradiation , solvent , microwave , condensation , condensation reaction , salicylic acid , spectroscopy , organic chemistry , nuclear chemistry , combinatorial chemistry , catalysis , biochemistry , physics , quantum mechanics , thermodynamics

Condensation reaction has been carried out for the synthesis of some N'-benzylidene-2-hydroxybenzohydrazides using microwave assisted solvent-free method. The structures of all the products obtained in the present work are supported by spectral and analytical data (UV, IR, and 1H-NMR spectroscopy). The desired hydrazides are in 62-80% yields under microwave irradiation. The reaction was completed in 8-10 min.

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