Open AccessRAPID SOLVENT-FREE MICROWAVE ASSISTED SYNTHESIS OF SOME N’-BENZYLIDENE SALICYLIC ACID HYDRAZIDES
Author(s) -
Tutuk Budiati,
Stephanie D.A.,
Elisabeth Catherina Widjajakusuma
Publication year - 2012
Publication title -
indonesian journal of chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.273
H-Index - 14
eISSN - 2460-1578
pISSN - 1411-9420
DOI - 10.22146/ijc.21357
Subject(s) - chemistry , microwave irradiation , solvent , microwave , condensation , condensation reaction , salicylic acid , spectroscopy , organic chemistry , nuclear chemistry , combinatorial chemistry , catalysis , biochemistry , physics , quantum mechanics , thermodynamics
Condensation reaction has been carried out for the synthesis of some N'-benzylidene-2-hydroxybenzohydrazides using microwave assisted solvent-free method. The structures of all the products obtained in the present work are supported by spectral and analytical data (UV, IR, and 1H-NMR spectroscopy). The desired hydrazides are in 62-80% yields under microwave irradiation. The reaction was completed in 8-10 min.