Open AccessSynthesis and Characterization of New Polyimide by Curing Poly Acryloyl Chloride with Different Amides
Author(s) -
Baghdad Science Journal
Publication year - 2013
Publication title -
mağallaẗ baġdād li-l-ʿulūm
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.167
H-Index - 6
eISSN - 2411-7986
pISSN - 2078-8665
DOI - 10.21123/bsj.10.3.686-698
Subject(s) - acryloyl chloride , polyimide , polymer , solubility , solvent , curing (chemistry) , polymer chemistry , amine gas treating , melting point , isopropyl , chloride , materials science , chemistry , organic chemistry , monomer , layer (electronics) , acrylate
The present work involved preparation of new substituted and unsubstituted and poly imides (1-17) using reaction of acryloyl chloride with different amides (aliphatic ,aromatic) in the presence of a suitable solvent and amount tri ethyl amine (Et3N) with heating – the structure confirmation of all polymers were proved using FT-IR,1H-NMR,C13NMR and UV spectroscopy ,thermal analysis (TG) for some polymers confirmed their thermal stabilities . Other physical properties including softening and melting points, PH and solubility of the polymers were also measured