Open AccessThe Effect of Bioactive Glass and Sintering Conditions on the Properties of Titanium-Hydroxyapatite Composites
Author(s) -
Mohamed Abdulmunem,
Muralithran G. Kutty,
Wan Haliza Abd Majid,
Ali Dabbagh,
Noor Hayaty Abu Kasim,
Noor Azlin Yahya,
Hadijah Abdullah
Publication year - 2021
Publication title -
sains malaysiana
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.251
H-Index - 29
eISSN - 2735-0118
pISSN - 0126-6039
DOI - 10.17576/jsm-2021-5004-19
Subject(s) - sintering , materials science , titanium , decomposition , composite material , bioactive glass , composite number , indentation hardness , microstructure , metallurgy , chemistry , organic chemistry
Titanium-hydroxyapatite (Ti-HA) based composites have been widely investigated as viable materials to be used in dentistry. However, sintering of these composites is very challenging due to decomposition of HA and oxidation of Ti. The objective of this study was to investigate the effect of incorporating a bioactive glass in Ti-HA composites sintered in different atmospheric conditions. The bioactive glass was prepared and added to different percentages of Ti-HA mixtures and divided into two groups. Samples in Group 1 were sintered with air atmosphere, while samples in Group 2 were sintered with vacuum furnace. All samples were later subjected to XRD, SEM, density, micro-hardness, and compression strength tests. XRD results showed that in Group 1, the major phases were assigned to Ti and HA while the minor phases were assigned to oxidised Ti. Whereas, Group 2 showed that the major phases were assigned to HA and the minor phases showed decomposition of HA to Ca3(PO4)2(TCP) and Ca4(PO4)2O (TTCP). Oxidized Ti was also present in this group. In terms of density, micro-hardness and compression strength, statistical analyses showed that samples in Group 1 have a significant difference (p = 0.000) as compared to those in Group 2. Sintering Ti-HA composites incorporated with BGby using air atmosphere furnace could reduce the decomposition of HA and oxidation of Ti, thus improve the density, micro-hardness and compression strength of the composites.