Open AccessCHARACTERISTIC OF XONOTLITE SYNTHESIZED BY HYDROTHERMAL REACTION USING RICE HUSK ASH AND ITS APPLICATION TO ABSORB CHROME (III) SOLUTION
Author(s) -
Trung Kien Pham,
Tran Ngo Quan
Publication year - 2021
Publication title -
materiali in tehnologije
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.27
H-Index - 25
eISSN - 1580-3414
pISSN - 1580-2949
DOI - 10.17222/mit.2021.233
Subject(s) - husk , materials science , hydrothermal circulation , scanning electron microscope , nuclear chemistry , chromium , adsorption , chemical engineering , mineralogy , metallurgy , chemistry , composite material , botany , organic chemistry , engineering , biology
In this paper, we report on synthesizing xonotlite, calcium silicate hydrate (CSH), via a hydrothermal reaction using rice husk from the Mekong Delta, Vietnam. The rice husks were burnt at 1000 °C for 3 h. Grey rice husk ash was collected, then mixed with Ca(OH)2 at a Ca/Si molar ratio of 1 : 1. This was followed by a hydrothermal reaction at 180 °C for 24 h and 48 h to obtain the xonotlite mineral. Before and after adsorption, 3-mm xonotlite pellets were thoroughly characterized using X-ray diffractometry (XRD), X-ray fluorescence (XRF), scanning electron microscopy (SEM) and ultraviolet-visible (UV-VIS) spectroscopy. This material has potential application in chromium(III) removal during a chrome-plating process. The adsorption efficiency of the 3-mm pellet samples reached more than 76 % after 12 h.