Open AccessA facile hydrothermal approach for catalytic and optical behavior of tin oxide- graphene (SnO2/G) nanocomposite
Author(s) -
Suresh Sagadevan,
Zaira Zaman Chowdhury,
Mohd Rafie Johan,
Ali Akbar Khan,
Fauziah Abdul Aziz,
Rahman Faizur Rafique,
Enamul Hoque
Publication year - 2018
Publication title -
plos one
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.99
H-Index - 332
ISSN - 1932-6203
DOI - 10.1371/journal.pone.0202694
Subject(s) - graphene , materials science , nanocomposite , photocatalysis , raman spectroscopy , tin oxide , high resolution transmission electron microscopy , nanoparticle , chemical engineering , hydrothermal circulation , fourier transform infrared spectroscopy , oxide , nanotechnology , composite material , catalysis , transmission electron microscopy , chemistry , organic chemistry , optics , physics , engineering , metallurgy
A cost-effective, facile hydrothermal approach was made for the synthesis of SnO 2 /graphene (Gr) nano-composites. XRD diffraction spectra clearly confirmed the presence of tetragonal crystal system of SnO 2 which was maintaining its structure in both pure and composite materials’ matrix. The stretching and bending vibrations of the functional groups were analyzed using FTIR analysis. FESEM images illustrated the surface morphology and the texture of the synthesized sample. HRTEM images confirmed the deposition of SnO 2 nanoparticles over the surface of graphene nano-sheets. Raman Spectroscopic analysis was carried out to confirm the in-plane blending of SnO 2 and graphene inside the composite matrix. The photocatalytic performance of the synthesized sample under UV irradiation using methylene blue dye was observed. Incorporation of grapheme into the SnO 2 sample had increased the photocatalytic activity compared with the pure SnO 2 sample. The electrochemical property of the synthesized sample was evaluated.