Spray Pyrolysis Technique for the deposition of Lead Oxide (PbO) Thin Films; its Electrochemical behaviour and Structural and optical Properties | Zendy

Anil B. Gite | Zendy; G. E. Patil | Zendy; G. H. Jain | Zendy

Open Access

Spray Pyrolysis Technique for the deposition of Lead Oxide (PbO) Thin Films; its Electrochemical behaviour and Structural and optical Properties

Author(s) -

Anil B. Gite,

G. E. Patil,

G. H. Jain

Publication year - 2018

Publication title -

material science research india

Language(s) - English

Resource type - Journals

eISSN - 2394-0565

pISSN - 0973-3469

DOI - 10.13005/msri/150204

Subject(s) - lead oxide , materials science , cyclic voltammetry , thin film , oxide , platinum , electrode , deposition (geology) , substrate (aquarium) , spray pyrolysis , electrochemistry , working electrode , pyrolysis , chemical engineering , analytical chemistry (journal) , inorganic chemistry , nanotechnology , metallurgy , chemistry , catalysis , organic chemistry , paleontology , sediment , geology , engineering , oceanography , biology

Thin film of Lead oxide (PbO) was prepared by spray pyrolysis technique on glass substrate at 250°C. The cyclic voltammetry measurement was carried out to study the oxidation reduction reactions of non-aqueous lead ions at various molar concentrations which is from 0.01M to 0.09M. Elecrochemical studies were carried out with Ag/AgCl as a reference electrode , Pt as working electrode while platinum mesh as counter electrode.Lead oxide appears to be poisonous yellow or reddish yellow solid. Structural characterization of films was analyze with X- ray diffraction (XRD) and optical band gap was determined by UV-Vis Spectroscopy.

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