Open AccessPreparation and Characterization of the Schiff Base Ligand (E)- N-(3-nitrobenzylidene) isonicotinohydrazide and its Silver (I) Complex [Ag(NNBIH)2]+
Author(s) -
Shahriar Ghammamy,
Sajjad Sedaghat
Publication year - 2012
Publication title -
material science research india/material science research india
Language(s) - English
Resource type - Journals
eISSN - 2394-0565
pISSN - 0973-3469
DOI - 10.13005/msri/090203
Subject(s) - schiff base , ligand (biochemistry) , thermal decomposition , chemistry , thermal analysis , characterization (materials science) , metal , infrared spectroscopy , differential thermal analysis , spectroscopy , base (topology) , inorganic chemistry , polymer chemistry , nuclear chemistry , materials science , organic chemistry , thermal , nanotechnology , diffraction , biochemistry , receptor , mathematical analysis , physics , mathematics , quantum mechanics , meteorology , optics
We describe the synthesis and characterization of a new silver (I) complex of the Schiff base ligand (E) - N-(3-nitrobenzylidene) is onicotinohydrazide that abbreviated as NNBIH was synthesized and characterized. Ag (I) Metal complex of this Schiff base ligand prepared by reaction of nitrate salt of Ag (I) with NNBIH. Characterization of the ligand was made by microanalyses, FT-IR, UV–Visible spectroscopy and its complex was made by microanalyses, FT-IR and UV–Visible spectroscopy. TG- DTA and other analytical methods have been applied to the investigation of the thermal behavior and Structure of the compound [Ag(NNBIH)2]+. Thermal decomposition of these compounds is multistage processes.