Melamine Trisulfonic Acid: An Efficient, Heterogeneous and Reusable Catalyst for the Synthesis of 10‐Aryl‐6,8‐dimethyl‐ 6, 10‐dihydro‐5‐oxa‐6,8‐diazaanthra [2,3‐d][1,3]dioxole‐ 7,9‐diones
Author(s) -
Weilin Li,
QiuYan Luo
Publication year - 2011
Publication title -
journal of chemistry
Language(s) - English
Resource type - Journals
eISSN - 2090-9063
pISSN - 2090-9071
DOI - 10.1155/2011/853747
Subject(s) - chemistry , melamine , catalysis , aryl , methylene , condensation , organic chemistry , solvent , condensation reaction , solid acid , alkyl , physics , thermodynamics
Melamine trisulfonic acid was used as an efficient and recyclable catalyst for the one-pot synthesis of 10-aryl-6,8-dimethyl-6,10-dihydro-5-oxa-6,8-diazaanthra[2,3-d][1,3]dioxole-7,9-diones by condensation of 3,4-methylene dioxyphenol, aromatic aldehydes and 1,3-dimethylbarbituric acid under solvent-free conditions. Different types of aromatic. aldehydes were used in the reaction and in all cases the products were obtained in good to excellent yields
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