Synthesis of 8-, 9-, 12-, and 13-mono-13C-retinal
Author(s) -
Johannes A. Pardoen,
Peter Mulder,
E. M. M. van den Berg,
Johan Lugtenburg
Publication year - 1985
Publication title -
canadian journal of chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.323
H-Index - 68
eISSN - 1480-3291
pISSN - 0008-4042
DOI - 10.1139/v85-246
Subject(s) - chemistry , acetonitrile , retinal , coupling constant , stereochemistry , organic chemistry , biochemistry , physics , particle physics
The 8-, 9-, 12-, and 13-mono- 13 C-retinals were synthesized with > 98% chemical purity and 93% 13 C incorporation from 13 C-labelled acetonitrile. Their 13 C– 13 C and 13 C– 1 H nmr coupling constants were determined.
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