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Preparation and high‐temperature oxidation resistance of multilayer MoSi 2 /MoB coating by spent MoSi 2 ‐based materials
Author(s) -
Zhu Lu,
Wang Xiaohong,
Ren Xuanru,
Kang Xueqin,
Akhtar Farid,
Feng Peizhong
Publication year - 2021
Publication title -
journal of the american ceramic society
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.9
H-Index - 196
eISSN - 1551-2916
pISSN - 0002-7820
DOI - 10.1111/jace.17723
Subject(s) - materials science , coating , sintering , layer (electronics) , oxide , diffusion , substrate (aquarium) , metallurgy , slurry , composite material , oceanography , physics , thermodynamics , geology
Spent MoSi 2 and MoB were used as raw materials to prepare multilayer MoSi 2 /MoB coating on molybdenum by the two‐step method of slurry deposition and spark plasma sintering. The results showed dense MoSi 2 /MoB coating after sintering while penetrated cracks appeared in MoSi 2 coating due to coefficient of thermal expansion mismatch between the Mo substrate and coating. After the sintering of MoSi 2 /MoB coatings, MoB and Mo 2 B diffusion layers were formed between MoB transition layer and Mo substrate without defects, exhibiting good metallurgical bonding. The high‐temperature oxidation behavior of coatings (1500°C) was also explored. After oxidation of 50 h at 1500°C, lowest mass gain (0.035 mg/cm 2 ) was obtained for MoSi 2 /MoB coating, and the oxide scale was dense and complete without voids, making the oxygen diffusion at elevated temperature inhibited. Compared with MoSi 2 coating under the same oxidation conditions, relatively thinner silica oxide scale was acquired by MoSi 2 /MoB coating because of the reduction of cracks, and the multilayer coating exhibits better anti‐oxidation properties at high temperature.

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