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3D printing of dense structural ceramic microcomponents with low cost: Tailoring the sintering kinetics and the microstructure evolution
Author(s) -
Liu Wei,
Wu Haidong,
Tian Zhuo,
Li Yanhui,
Zhao Zhe,
Huang Meipeng,
Deng Xin,
Xie Zhipeng,
Wu Shanghua
Publication year - 2019
Publication title -
journal of the american ceramic society
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.9
H-Index - 196
eISSN - 1551-2916
pISSN - 0002-7820
DOI - 10.1111/jace.16241
Subject(s) - sintering , materials science , ceramic , microstructure , stereolithography , microelectromechanical systems , grain size , grain growth , composite material , nanotechnology
Abstract In this study, we have successfully developed a unique 3D printing approach based on mask‐image‐projection stereolithography ( MIP ‐ SL ) to fabricate structural ceramics microcomponents with low cost and high efficiency. Ultra‐dense submicron crystalline ceramics without fierce grain growth could be obtained via tailoring the sintering kinetics. The ZrO 2 ceramic microcomponents reached the highest relative density ( RD ) of 99.7% with the average grain size of 0.52 μm upon sintering at 1550°C while the Al 2 O 3 ceramic microcomponents reached its highest RD of 98.31% with the average grain size of 2.6 μm upon sintering at 1600°C. Oxide ceramics microcomponents of fully flexible design can be produced easily without visible defects via the method developed in this study, which demonstrates significant potential in the applications of microelectromechanical systems, micro‐optical electronics systems and micro‐opto‐electro‐mechanical systems. The method developed in this study has addressed the problem successfully by healing the interlayer interface defects in densification process via the sintering kinetic window and microstructure evolution. The current work provides a promising opportunity to fabricate structural ceramic microcomponents with complex shape, high precision, and high surface smoothness.