Flash Spark Plasma Sintering ( FSPS ) of Pure   ZrB   2 | Zendy

Grasso Salvatore | Zendy; Saunders Theo | Zendy; Porwal Harshit | Zendy; CedillosBarraza Omar | Zendy; Jayaseelan Daniel Doni | Zendy; Lee William E. | Zendy; Reece Mike John | Zendy

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Flash Spark Plasma Sintering ( FSPS ) of Pure ZrB 2

Author(s) -

Grasso Salvatore,

Saunders Theo,

Porwal Harshit,

CedillosBarraza Omar,

Jayaseelan Daniel Doni,

Lee William E.,

Reece Mike John

Publication year - 2014

Publication title -

journal of the american ceramic society

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.9

H-Index - 196

eISSN - 1551-2916

pISSN - 0002-7820

DOI - 10.1111/jace.13109

Subject(s) - spark plasma sintering , materials science , microstructure , ceramic , sintering , composite material , flash (photography) , carbide , art , visual arts

Pure ZrB 2 powder was Flash sintered in an SPS furnace ( FSPS ). The samples were densified up to 95.0% in 35 s under an applied pressure of 16 MPa. Compared to Conventional SPS ( CSPS ), the newly developed FSPS technique resulted in an unprecedented energy and time savings of about 95% and 98% respectively. ZrB 2 monoliths obtained by CSPS and FSPS were compared with respect to microstructures, densification behavior, and grain growth. The developed methodology might find application to a wide range of highly conductive ceramics as such refractory borides and carbides.

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