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Glass–Ceramic Composites with Strontium Hexaferrite Ultrafine Particles in the SrO–Fe 2 O 3 –B 2 O 3 –SiO 2 System
Author(s) -
Zaitsev Dmitry D.,
Gravchikova Ekaterina A.,
Kazin Pavel E.,
Tretyakov Yury D.,
Jansen Martin
Publication year - 2006
Publication title -
international journal of applied ceramic technology
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.4
H-Index - 57
eISSN - 1744-7402
pISSN - 1546-542X
DOI - 10.1111/j.1744-7402.2006.02093.x
Subject(s) - materials science , devitrification , ceramic , coercivity , strontium , composite material , analytical chemistry (journal) , mineralogy , crystallization , chemical engineering , chemistry , chromatography , physics , engineering , condensed matter physics , nuclear physics
Glass samples with nominal compositions SrFe 12 O 19 +(12− n )SrB 2 O 4 +nSrSiO 3 , n =3, 6, 9 were prepared by rapid quenching of the melt. Processes of glass devitrification were studied. The samples were annealed at temperatures of 600–900°C, and the resulting glass–ceramics was characterized by XRD, SEM, EDX, and magnetic measurements. SrFe 12 O 19 crystallizes above 700°C and forms nano‐ and submicron platelet particles with the aspect ratio depending on the thermal treatment conditions. The glass–ceramic samples annealed at 900°C show coercive force values in the range of 422–455 kA/m.