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Effect of the addition of silanated silica on the mechanical properties of microwave heat‐cured acrylic resin
Author(s) -
da Silva Lucas H.,
Feitosa Sabrina A.,
Valera Marcia C.,
de Araujo Maria A.M.,
Tango Rubens N.
Publication year - 2012
Publication title -
gerodontology
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.7
H-Index - 54
eISSN - 1741-2358
pISSN - 0734-0664
DOI - 10.1111/j.1741-2358.2011.00604.x
Subject(s) - flexural strength , acrylic resin , vickers hardness test , composite material , silane , materials science , hardness , polymerization , microstructure , polymer , coating
doi: 10.1111/j.1741‐2358.2011.00604.x
Effect of the addition of silanated silica on the mechanical properties of microwave heat‐cured acrylic resin Objectives: The purpose of this study was to evaluate fthe flexural strength and Vickers hardness of a microwave energy heat‐cured acrylic resin by adding different concentrations of silane surface‐treated nanoparticle silica. Methods: Acrylic resin specimens with dimensions of 65 × 10 × 2.5 mm were formed and divided into five experimental groups ( n = 10) according to the silica concentration added to the acrylic resin mass (weight %) prior to polymerisation : G1, without silica; G2, 0.1% silica; G3, 0.5% silica; G4, 1.0% silica; and G5, 5.0% silica. The specimens were submitted to a three‐point flexural strength test and to the Vickers hardness test (HVN). The data obtained were statistically analysed by anova and the Tukey test (α = 0.05). Results: Regarding flexural strength, G5 differed from the other experimental groups (G1, G2, G3 and G4) presenting the lowest mean, while G4 presented a significantly higher mean, with the exception of group G3. Regarding Vickers hardness, a decrease in values was observed, in which G1 presented the highest hardness compared with the other experimental groups. Conclusion: Incorporating surface‐treated silica resulted in direct benefits in the flexural strength of the acrylic resin activated by microwave energy; however, similar results were not achieved for hardness.