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Effect of Stepped Light Intensity on Polymerization Force and Conversion in a Photoactivated Composite
Author(s) -
BOUSCHLICHER MURRAY R.,
RUEGGEBERG FREDERICK A.,
BOYER DANIEL B.
Publication year - 2000
Publication title -
journal of esthetic and restorative dentistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.919
H-Index - 60
eISSN - 1708-8240
pISSN - 1496-4155
DOI - 10.1111/j.1708-8240.2000.tb00195.x
Subject(s) - composite number , materials science , polymerization , curing (chemistry) , composite material , fourier transform infrared spectroscopy , shrinkage , analytical chemistry (journal) , chemistry , optics , polymer , physics , chromatography
Purpose : This study evaluated the effect of stepped light intensity on the polymerization shrinkage forces and degrees of conversion of a hybrid composite. Materials and Methods: Composite specimens were bonded between two steel rods (5.00 mm diameter, 1.25 mm apart, configuration factor = 2) mounted in a universal testing machine using a constant displacement mode. Polymerization contraction force was recorded for 300 seconds under four light exposure conditions: group 1: 40 s × 800 mW/cm 2 ; group 2: 10 s × 100 mW/cm 2 + 30 s × 800 mW/cm 2 ; group 3: 60 s × 800 mW/cm 2 ; group 4: 10 s × 100 mW/cm 2 + 50 s × 800 mW/cm 2 . Maximum curing force (N 300s ) and maximum force rate of the four groups were compared using one‐way analysis of variance (ANOVA) (α= 0.05) and the Tukey test. Degree of conversion in all groups was evaluated at two depths (top surface and 2 mm) using Fourier transform infrared spectroscopy (FTIR). Results: Mean maximum shrinkage forces and standard deviations (SD) were: group 1, 177 N (SD = 23); group 2, 172 N (SD = 11); group 3, 213 N (SD = 15); group 4, 197 N (SD = 17). Mean maximum forces for stepped and standard groups with the same duration (1 and 2; 3 and 4) were not statistically different; means for groups 2 and 3 were statistically different. Maximum force rates were not significantly different ( p = .1548). Force:time curves were S‐shaped. Specimens exposed to stepped curing exhibited longer delays before force was recorded. Mode of curing was shown not to contribute to overall cure, but both duration of cure and the depth (top surface vs. 2.00 mm) were significant with an interaction effect. CLINICAL SIGNIFICANCE Mean maximum shrinkage force and force rate exhibited during the first 300 seconds of polymerization were not influenced by using stepped light exposure. Degree of conversion was equivalent for exposures of similar total duration at 2‐mm depth. Mode of cure (stepped vs. continuous intensity) had no effect on degree of conversion.
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