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Surface free‐energy measurements as indicators of the bonding characteristics of single‐step self‐etching adhesives
Author(s) -
Inoue Naoki,
Tsujimoto Akimasa,
Takimoto Masayuki,
Ootsuka Eiichiro,
Endo Hajime,
Takamizawa Toshiki,
Miyazaki Masashi
Publication year - 2010
Publication title -
european journal of oral sciences
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.802
H-Index - 93
eISSN - 1600-0722
pISSN - 0909-8836
DOI - 10.1111/j.1600-0722.2010.00771.x
Subject(s) - adhesive , dentin , materials science , composite material , surface energy , surface roughness , distilled water , bond strength , single bond , etching (microfabrication) , contact angle , chemistry , layer (electronics) , alkyl , organic chemistry , chromatography
Inoue N, Tsujimoto A, Takimoto M, Ootsuka E, Endo H, Takamizawa T, Miyazaki M. Surface free‐energy measurements as indicators of the bonding characteristics of single‐step self‐etching adhesives.
Eur J Oral Sci 2010; 118: 525–530. © 2010 Eur J Oral Sci This study examined the surface free‐energy of dentin treated with the single‐step self‐etching adhesives Bond Force, Clearfil tri‐S Bond, and G‐Bond Plus. The labial dentin surfaces of bovine mandibular incisors were wet ground with #180‐, #600‐, and #2,000‐grit silicon carbide paper. The adhesives were applied to the ground dentin, and then rinsed with acetone and distilled water. The surface free‐energies were determined by measuring the contact angles of three test liquids placed on the adhesive‐treated dentin. The surface free‐energies of the samples treated with the G‐Bond Plus and Clearfil tri‐S Bond adhesives increased as the surface roughness decreased. No significant differences in the surface free‐energy were found for the samples treated with the Bond Force adhesive, regardless of the surface roughness. These results indicated that dentin surfaces treated with adhesives did not promote a higher surface‐energy state, and that differences in the components of surface energy were apparent for the adhesives tested.