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Microwave Sintering of Nanocrystalline Ni 1− x Zn x Fe 2 O 4 Ferrite Powder and Their Magnetic Properties
Author(s) -
Liu Yin,
Yi Zhiguo,
Li Jianjun,
Qiu Tai,
Min Fanfei,
Zhang Mingxu
Publication year - 2013
Publication title -
journal of the american ceramic society
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.9
H-Index - 196
eISSN - 1551-2916
pISSN - 0002-7820
DOI - 10.1111/j.1551-2916.2012.05437.x
Subject(s) - nanocrystalline material , materials science , sintering , microstructure , ferrite (magnet) , coprecipitation , grain size , analytical chemistry (journal) , microwave , metallurgy , ceramic , magnetization , composite material , inorganic chemistry , magnetic field , nanotechnology , chemistry , physics , quantum mechanics , chromatography
Nanocrystalline Ni 1− x Zn x Fe 2 O 4 (0 ≤ x ≤ 1.0) powder with grain size of 30 nm was prepared using the spraying‐coprecipitation method. The obtained nanocrystalline Ni 1− x Zn x Fe 2 O 4 powder was sintered using conventional and microwave sintering techniques. The results show that the microstructure and magnetic properties of the sintered samples are obviously improved by microwave sintering of nanocrystalline Ni 1− x Zn x Fe 2 O 4 ferrite powder. The initial permeability of Ni 1− x Zn x Fe 2 O 4 ferrite increases with the increase in zinc concentration, although its resonance frequencies shift from high frequency to low frequency. The maximum initial permeability for microwave‐sintered Ni 0.4 Zn 0.6 Fe 2 O 4 ceramic obtained at the temperature of 1170°C for 30 min reaches up to 360.9, and its resonance frequency is ~10 MHz. It may be attributed to the nanocrystalline Ni 1− x Zn x Fe 2 O 4 raw powder as well as the microwave sintering process, which results in a synergistic effect on improvement of the microstructure and magnetic properties.