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Preparation of a Dense/Porous BiLayered Ceramic by Applying an Electric Field During Freeze Casting
Author(s) -
Zhang Yumin,
Hu Luyang,
Han Jiecai
Publication year - 2009
Publication title -
journal of the american ceramic society
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.9
H-Index - 196
eISSN - 1551-2916
pISSN - 0002-7820
DOI - 10.1111/j.1551-2916.2009.03110.x
Subject(s) - electric field , materials science , porosity , ceramic , slurry , sintering , composite material , tape casting , casting , intensity (physics) , dielectric , optics , optoelectronics , physics , quantum mechanics
Dense/porous bilayered ceramics were fabricated by introducing an electric field into the freeze‐casting process. A unidirectional solidification was performed by placing an aqueous ceramic on refrigerating equipment, at a constant cooling rate of 6°C/min. When the bottom temperature of the slurry was reduced to 0°C, an electric field along the vertical direction was applied until the freezing process was completed. After drying and sintering of the green part, an as‐prepared ceramic with dense/porous bilayered architectures was obtained. It was shown that the thickness of the dense layer in the sample could be controlled by tuning the electric field intensity from 51 to 155 μm as the electric field increased from 15 to 90 V. On the other hand, all samples exhibited almost an identical lamellae thickness and interlayer distance in the porous region, as large as ∼14 and ∼24 μm, respectively.