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TEM foil preparation of sub‐micrometre sized individual grains by focused ion beam technique
Author(s) -
HOLZAPFEL C.,
SOLDERA F.,
VOLLMER C.,
HOPPE P.,
MÜCKLICH F.
Publication year - 2009
Publication title -
journal of microscopy
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.569
H-Index - 111
eISSN - 1365-2818
pISSN - 0022-2720
DOI - 10.1111/j.1365-2818.2009.03181.x
Subject(s) - transmission electron microscopy , foil method , focused ion beam , materials science , microscopy , energy filtered transmission electron microscopy , scanning electron microscope , grain size , conventional transmission electron microscope , scanning transmission electron microscopy , analytical chemistry (journal) , nanotechnology , ion , optics , chemistry , composite material , physics , chromatography , organic chemistry
Summary Analysis of presolar silicate grains provides new knowledge on interstellar and circumstellar environments and can be used to test models of the Galactic chemical evolution. However, structural information of these grains is rare because sample preparation for transmission electron microscopy is very difficult due to the small dimensions of these grains (<0.5 μm). With the use of the focused ion beam technique thin foils from these grains for transmission electron microscopy analysis can be prepared. Nevertheless, reaching the required precision of some tens of nanometres for the preparation of the transmission electron microscopy foil in the place of interest is not trivial. Furthermore, in the current samples, the grain of interest can only be identified by its different isotopic composition; i.e. there is no contrast difference in scanning electron microscopy or transmission electron microscopy images which allow the identification of the grain. Therefore, the grain has to be marked in some way before preparing the transmission electron microscopy foil. In the present paper, a method for transmission electron microscopy foil preparation of grains about 200 to 400 nm in diameter is presented. The method utilizes marking of the grain by Pt deposition and milling of holes to aid in the exact orientation of the transmission electron microscopy foil with respect to the grain. The proposed method will be explained in detail by using an example grain.