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Mass Spectrometric Analysis of Bubbles in Glass
Author(s) -
SHICK RICHARD L.,
SWARTS E. LOWELL
Publication year - 1982
Publication title -
journal of the american ceramic society
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.9
H-Index - 196
eISSN - 1551-2916
pISSN - 0002-7820
DOI - 10.1111/j.1151-2916.1982.tb09935.x
Subject(s) - mass spectrometry , calibration , analytical chemistry (journal) , quadrupole , quadrupole mass analyzer , chemistry , materials science , chromatography , physics , atomic physics , quantum mechanics
Procedures have been developed for analyzing, by quadrupole mass spectrometry, gases contained in bubbles within glass. Commonly sought‐for species are detected individually at minimum levels of 3 to 70x10 −4 nL (STP) in bubbles 0.1 to 1 mm in diameter. Calibration is obtained by analyzing certified gas mixtures contained in glass capillaries at known pressures and volumes.