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Preparation and properties of porous SiC–Al 2 O 3 ceramics using coal ash
Author(s) -
Yin Yue,
Ma Beiyue,
Hu Chuanbo,
Liu Guoqi,
Li Hongxia,
Su Chang,
Ren Xinming,
Yu Jingyu,
Zhang Yaran,
Yu Jingkun
Publication year - 2018
Publication title -
international journal of applied ceramic technology
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.4
H-Index - 57
eISSN - 1744-7402
pISSN - 1546-542X
DOI - 10.1111/ijac.13080
Subject(s) - materials science , porosity , thermal shock , ceramic , microstructure , thermal diffusivity , compressive strength , composite material , carbothermic reaction , chemical engineering , carbide , physics , quantum mechanics , engineering
In this paper, we first reported that porous SiC–Al 2 O 3 ceramics were prepared from solid waste coal ash, activated carbon, and commercial SiC powder by a carbothermal reduction reaction ( CRR ) method under Ar atmosphere. The effects of addition amounts of SiC (0, 10, 15, and 20 wt%) on the postsintering properties of as‐prepared porous SiC–Al 2 O 3 ceramics, such as phase composition, microstructure, apparent porosity, bulk density, pore size distribution, compressive strength, thermal shock resistance, and thermal diffusivity have been investigated. It was found that the final products are β‐SiC and α‐Al 2 O 3 . Meanwhile, the SEM shows the pores distribute uniformly and the body gradually contacts closely in the porous SiC–Al 2 O 3 ceramics. The properties of as‐prepared porous SiC–Al 2 O 3 ceramics were found to be remarkably improved by adding proper amounts of SiC (10, 15, and 20 wt%). However, further increasing the amount of SiC leads to a decrease in thermal shock resistance and mechanical properties. Porous SiC–Al 2 O 3 ceramics doped with 10 wt% SiC and sintered at 1600°C for 5 hours with the median pore diameter of 4.24 μm, room‐temperature compressive strength of 21.70 MP a, apparent porosity of 48%, and thermal diffusivity of 0.0194 cm 2 /s were successfully obtained.