
Simultaneous X‐ray radioscopy/tomography and energy‐dispersive diffraction applied to liquid aluminium alloy foams
Author(s) -
Jiménez Catalina,
Paeplow Marlen,
Kamm Paul H.,
Neu Tillmann R.,
Klaus Manuela,
Wagener Guido,
Banhart John,
Genzel Christoph,
García-Moreno Francisco
Publication year - 2018
Publication title -
journal of synchrotron radiation
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.172
H-Index - 99
ISSN - 1600-5775
DOI - 10.1107/s1600577518011657
Subject(s) - materials science , tomography , synchrotron radiation , diffraction , alloy , synchrotron , x ray , aluminium , optics , x ray crystallography , composite material , physics
High‐speed X‐ray imaging in two dimensions (radioscopy) and three dimensions (tomography) is combined with fast X‐ray diffraction in a new experimental setup at the synchrotron radiation source BESSY II. It allows for in situ studies of time‐dependent phenomena in complex systems. As a first application, the foaming process of an aluminium alloy was studied in three different experiments. Radioscopy, optical expansion measurements and diffraction were used to correlate the change of foam morphology to the various phases formed during heating of an AlMg15Cu10 alloy to 620°C in the first experiment. Radioscopy was then replaced by tomography. Acquiring tomograms and diffraction data at 2 Hz allows even more details of foam evolution to be captured, for example, bubble size distribution. In a third experiment, 4 Hz tomography yields dynamic insights into fast phenomena in evolving metal foam.