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A novel high‐throughput setup for in situ powder diffraction on coin cell batteries
Author(s) -
Herklotz Markus,
Weiß Jonas,
Ahrens Eike,
Yavuz Murat,
Mereacre Liuda,
Kiziltas-Yavuz Nilüfer,
Dräger Christoph,
Ehrenberg Helmut,
Eckert Jürgen,
Fauth Francois,
Giebeler Lars,
Knapp Michael
Publication year - 2016
Publication title -
journal of applied crystallography
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.429
H-Index - 162
ISSN - 1600-5767
DOI - 10.1107/s1600576715022165
Subject(s) - in situ , spinel , diffraction , electrode , materials science , synchrotron , electrochemistry , powder diffraction , electrochemical cell , battery (electricity) , throughput , analytical chemistry (journal) , optics , computer science , crystallography , chemistry , metallurgy , physics , chromatography , telecommunications , power (physics) , organic chemistry , quantum mechanics , wireless
A new setup for in situ experiments with up to eight electrochemical cells, especially battery coin cells, and the corresponding custom‐made in situ cells are presented. The setup is primarily optimized for synchrotron powder diffraction measurements. As a newly constructed experimental setup, the in situ coin cell holder was tested for positional errors of the cells and the reliability of the diffraction as well as electrochemical measurements. The overall performance characteristics of the sample holder are illustrated by measurements on LiMn 2 O 4 and LiNi 0.35 Fe 0.3 Mn 1.35 O 4 spinel‐based positive electrode materials.