Nitronium tetrafluoroborate | Zendy

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Nitronium tetrafluoroborate

Author(s) -

Krossing Ingo,

Raabe Ines,

Birtalan Esther

Publication year - 2007

Publication title -

acta crystallographica section e

Language(s) - English

Resource type - Journals

ISSN - 1600-5368

DOI - 10.1107/s1600536807000207

Subject(s) - tetrafluoroborate , boron , tetra , nitro , chemistry , medicinal chemistry , crystallography , inorganic chemistry , organic chemistry , ionic liquid , catalysis , alkyl

Commercially available nitronium tetrafluoroborate, NO 2 + ·BF 4 − , has been recrystallized from CH 2 Cl 2 as a side‐product of a reaction in which it has been used as a starting material. Both the NO 2 + cations and the BF 4 − anions are packed in considerably distorted cubic environments. The N=O distances of 1.1153 (8) and 1.1160 (7) Å as well as the O=N=O bond angle of 179.89 (7)° are similar to those found in other NO 2 + ‐containing salts described in the literature.

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