Structural studies of endohedral metallofullerenes by synchrotron radiation powder diffraction | Zendy

Nishibori E. | Zendy; Takata M. | Zendy; Sakata M. | Zendy; Shinohara H. | Zendy

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Structural studies of endohedral metallofullerenes by synchrotron radiation powder diffraction

Author(s) -

Nishibori E.,

Takata M.,

Sakata M.,

Shinohara H.

Publication year - 1998

Publication title -

journal of synchrotron radiation

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.172

H-Index - 99

ISSN - 1600-5775

DOI - 10.1107/s0909049597016816

Subject(s) - powder diffraction , synchrotron radiation , rietveld refinement , maximum entropy method , synchrotron , crystallography , materials science , diffraction , x ray crystallography , chemistry , physics , optics , crystal structure , computational physics

The endohedral natures of the metallofullerenes Y@C 82 and Sc 2 @C 8 4 are described based on synchrotron radiation powder diffraction experiments. For structural analysis, a combination of the maximum‐entropy method (MEM) and Rietveld refinement was employed to analyse the complicated powder pattern. The obtained MEM charge densities show a clear distinction of the endohedral natures of the mono‐ and dimetallofullerenes.

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