Development of µ‐PIC as a time‐resolved X‐ray area detector | Zendy

Takeda Atsushi | Zendy; Uekusa Hidehiro | Zendy; Kubo Hidetoshi | Zendy; Miuchi Kentaro | Zendy; Nagayoshi Tsutomu | Zendy; Ohashi Yuji | Zendy; Okada Yoko | Zendy; Orito Reiko | Zendy; Takada Atsushi | Zendy; Tanimori Toru | Zendy

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Development of µ‐PIC as a time‐resolved X‐ray area detector

Author(s) -

Takeda Atsushi,

Uekusa Hidehiro,

Kubo Hidetoshi,

Miuchi Kentaro,

Nagayoshi Tsutomu,

Ohashi Yuji,

Okada Yoko,

Orito Reiko,

Takada Atsushi,

Tanimori Toru

Publication year - 2005

Publication title -

journal of synchrotron radiation

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.172

H-Index - 99

ISSN - 1600-5775

DOI - 10.1107/s0909049505026713

Subject(s) - diffraction , detector , physics , optics , x ray , rotation (mathematics) , x ray detector , x ray crystallography , analytical chemistry (journal) , chemistry , computer science , artificial intelligence , chromatography

The application of a two‐dimensional micro‐pixel gas chamber (µ‐PIC) to X‐ray diffraction studies, and its performance, are reported. µ‐PIC has a 10 cm × 10 cm detection area, and a fast‐readout system for real‐time X‐ray imaging has been developed. Using the timing of each incoming X‐ray measured by µ‐PIC, continuous rotation photograph measurements were carried out for a 400 µm‐diameter spherical organic crystal of Ylid (C 11 H 10 O 2 S), and then diffraction spots were successfully obtained within 2θ of 49°. As a result, good internal agreement factors of 3.7% and 7.0% were confirmed among each of the symmetrically equivalent reflections for exposure times of 3700 s and 98 s, respectively.

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