(2 RS )‐4,4‐Dimethyl‐2‐[(1 SR )‐1‐phenylethyl]‐1‐pyrrolidinol | Zendy

Bernardinelli G. | Zendy; Oppolzer W. | Zendy; Spivey A. C. | Zendy

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(2 RS )‐4,4‐Dimethyl‐2‐[(1 SR )‐1‐phenylethyl]‐1‐pyrrolidinol

Author(s) -

Bernardinelli G.,

Oppolzer W.,

Spivey A. C.

Publication year - 1995

Publication title -

acta crystallographica section c

Language(s) - English

Resource type - Journals

eISSN - 1600-5759

pISSN - 0108-2701

DOI - 10.1107/s0108270194009686

Subject(s) - ring (chemistry) , pyrrolidine , stereospecificity , chemistry , molecule , hydroxylamine , stereochemistry , hydrogen bond , crystal structure , crystallography , organic chemistry , catalysis

In order to determine the stereospecificity of the Thermal cyclization of [(E)-2,2-dimethyl-5-phenyl-4- hexenyl] hydroxylamine (1), the relative configuration of the title compound, C₁₄H₂₁ NO, (2), has been established by single-crystal X-ray diffraction. The pyrrolidine ring adopts an envelope conformation with the N atom out of the ring plane. The molecules form hydrogen-bonded pairs through a centre of inversion [O...N 2.808 (5) A, and O---H...N 160 (4) °]

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