Low‐cost conversion of a coaxial nozzle arrangement into a stationary low‐temperature attachment | Zendy

Kottke T. | Zendy; Lagow R. J. | Zendy; Stalke D. | Zendy

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Low‐cost conversion of a coaxial nozzle arrangement into a stationary low‐temperature attachment

Author(s) -

Kottke T.,

Lagow R. J.,

Stalke D.

Publication year - 1996

Publication title -

journal of applied crystallography

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.429

H-Index - 162

ISSN - 1600-5767

DOI - 10.1107/s0021889896003172

Subject(s) - nozzle , coaxial , liquid nitrogen , atmospheric temperature range , materials science , range (aeronautics) , mechanics , mechanical engineering , chemistry , composite material , thermodynamics , physics , engineering , organic chemistry

A stationary nozzle accessory designed for the Siemens/Nicolet LTII low‐temperature device with standard ϕ ‐coaxial nozzle arrangement is described. The attachment is easy to assemble and its compatibility allows interchanging between both systems in less than 1 h, if required. Implementation of the stationary nozzle reduces the consumption of liquid nitrogen by more than 40% and extends the temperature range available for data collection by 60 K in the lower temperature range. Details of construction are presented, and a comparison with the ϕ ‐coaxial nozzle is discussed.

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