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Crystal data for an adduct of orthotelluric acid and urea, Te(OH) 6 .2CO(NH 2 ) 2
Author(s) -
Loub J.,
Dušek M.
Publication year - 1986
Publication title -
journal of applied crystallography
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.429
H-Index - 162
ISSN - 1600-5767
DOI - 10.1107/s0021889886089628
Subject(s) - diffractometer , raman spectroscopy , crystallography , adduct , crystal (programming language) , crystal structure , x ray crystallography , thermal decomposition , single crystal , urea , decomposition , diffraction , chemistry , materials science , analytical chemistry (journal) , physics , optics , organic chemistry , programming language , computer science
The crystal data of the title compound have been determined from single‐crystal data [Loub, Haase & Mergehenn (1979). Acta Cryst. B 35 , 3039–3041]: C 2/ c , a = 14.828(8), b = 8.891(6), c = 10.023(7) Å, β = 129.13(3)°, V = 1025.0(9) Å 3 , Z = 4, D m = 2.31(3), D x = 2.27 Mg m −3 . Power data obtained with powder diffractometer, θ –2 θ scan, T = 295 K, Cu K α radiation are presented. Infrared and Raman spectra are given. Thermal decomposition is reported [Fábry, Loub & Feltl (1982). J. Therm. Anal. 24 , 95–100]. The JCPDS Diffraction File No. for C 2 H 8 N 4 O 2 Te(OH) 6 is 36‐1470.