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Application of the X‐ray divergent‐beam technique for the determination of the angles between crystal blocks. II. Determination of the total misorientation angle between blocks
Author(s) -
Aristov V. V.,
Shmytko I. M.,
Shulakov E. V.
Publication year - 1974
Publication title -
journal of applied crystallography
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.429
H-Index - 162
ISSN - 1600-5767
DOI - 10.1107/s002188987401003x
Subject(s) - misorientation , beam (structure) , crystal (programming language) , optics , materials science , surface (topology) , geometry , crystallography , physics , chemistry , mathematics , computer science , microstructure , programming language , grain boundary
A method of determining the angles between the same planes in neighbouring blocks is described. The reflecting planes therefore may or may not coincide with the crystal surface. The method allows the determination of the total angle between the blocks from the divergent‐beam (DB) X‐ray patterns. The paper gives an example of the determination of the angles between blocks in an NaCl crystal. The experimental precision was 3′.