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Eine Methode zur Untersuchung extrem luftempfindlicher Substanzen mit der Guinier‐Methode
Author(s) -
Simon A.
Publication year - 1970
Publication title -
journal of applied crystallography
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.429
H-Index - 162
ISSN - 1600-5767
DOI - 10.1107/s0021889870005563
Subject(s) - capillary action , optics , monochromator , line (geometry) , materials science , physics , geometry , mathematics , wavelength , composite material
Powder patterns of an extremely air sensitive substance can be prepared in a modified Guinier type camera, the substance being introduced in a closed glass capillary. The capillary is situated on the focusing circle of the camera parallel to the focal line of the monochromator and is rotated during exposure to X‐rays. Line broadening and line shifts due to specimen geometry are discussed.